CARBAMIC ACID,N-METHYL-N-(2-OXOETHYL)-, 1,1-DIMETHYLETHYL ESTER
N-BOC-(METHYLAMINO)ACETALDEHYDE
CAS: 123387-72-4
Molecular Formula: C8H15NO3
CARBAMIC ACID,N-METHYL-N-(2-OXOETHYL)-, 1,1-DIMETHYLETHYL ESTER - Names and Identifiers
CARBAMIC ACID,N-METHYL-N-(2-OXOETHYL)-, 1,1-DIMETHYLETHYL ESTER - Physico-chemical Properties
| Molecular Formula | C8H15NO3 |
| Molar Mass | 173.21 |
| Density | 1.026g/ml |
| Boling Point | 218.2±19.0 °C(Predicted) |
| Flash Point | 85.781°C |
| Water Solubility | Slightly miscible with water. |
| Vapor Presure | 0.127mmHg at 25°C |
| pKa | -1.63±0.70(Predicted) |
| Storage Condition | Inert atmosphere,Store in freezer, under -20°C |
| Sensitive | Air Sensitive |
| Refractive Index | 1.44 |
| MDL | MFCD08064267 |
| Physical and Chemical Properties | Sensitivity: Air Sensitive |
| Use | This product is for scientific research only and shall not be used for other purposes. |
CARBAMIC ACID,N-METHYL-N-(2-OXOETHYL)-, 1,1-DIMETHYLETHYL ESTER - Introduction
N-Boc-(methylamino) acetaldehyde is a chemical compound whose chemical formula is C8H15NO3. The following are some properties, uses, preparation and safety information about N-Boc-(methylamino) acetaldehyde:
Nature:
-Appearance: Colorless to pale yellow oily liquid.
-Structure: The molecule contains a Boc group (tert-butoxycarbonyl) and a methylamine group (-NHCH3).
-Solubility: Soluble in alcohol, ether and aromatic hydrocarbon, insoluble in water.
-Stability: relatively stable to light and heat, but need to avoid contact with oxidants.
Use:
-Chemical synthesis intermediate: N-Boc-(methylamino) acetaldehyde is commonly used in organic synthesis as a precursor for the synthesis of α-amino aldehydes.
-Drug synthesis: It can be used to synthesize various drugs and bioactive molecules.
Preparation Method:
The preparation of N-Boc-(methylamino) acetaldehyde can be carried out by the following steps:
1. Methylamine (CH3NH2) and acetaldehyde (CH3CHO) are reacted in the presence of an acid catalyst.
2. After the synthesis is completed, the product is formed by adding trimethylolamine (trimethylamine) or participating in cyclopropane (cyclohexane) while removing ethanol.
3. Finally, N-Boc-(methylamino) acetaldehyde was obtained by extraction, separation and purification.
Safety Information:
- N-Boc-(Methylamino) acetaldehyde is an organic compound and needs to follow routine laboratory safety procedures when used.
-It may be irritating to the eyes, skin and respiratory system and direct contact should be avoided.
-Avoid inhaling or eating and maintain good ventilation.
-During use or storage, avoid contact with oxidants and strong acids to avoid dangerous reactions.
-When handling this compound, it is recommended to wear appropriate personal protective equipment, such as gloves, glasses and laboratory coats.
Nature:
-Appearance: Colorless to pale yellow oily liquid.
-Structure: The molecule contains a Boc group (tert-butoxycarbonyl) and a methylamine group (-NHCH3).
-Solubility: Soluble in alcohol, ether and aromatic hydrocarbon, insoluble in water.
-Stability: relatively stable to light and heat, but need to avoid contact with oxidants.
Use:
-Chemical synthesis intermediate: N-Boc-(methylamino) acetaldehyde is commonly used in organic synthesis as a precursor for the synthesis of α-amino aldehydes.
-Drug synthesis: It can be used to synthesize various drugs and bioactive molecules.
Preparation Method:
The preparation of N-Boc-(methylamino) acetaldehyde can be carried out by the following steps:
1. Methylamine (CH3NH2) and acetaldehyde (CH3CHO) are reacted in the presence of an acid catalyst.
2. After the synthesis is completed, the product is formed by adding trimethylolamine (trimethylamine) or participating in cyclopropane (cyclohexane) while removing ethanol.
3. Finally, N-Boc-(methylamino) acetaldehyde was obtained by extraction, separation and purification.
Safety Information:
- N-Boc-(Methylamino) acetaldehyde is an organic compound and needs to follow routine laboratory safety procedures when used.
-It may be irritating to the eyes, skin and respiratory system and direct contact should be avoided.
-Avoid inhaling or eating and maintain good ventilation.
-During use or storage, avoid contact with oxidants and strong acids to avoid dangerous reactions.
-When handling this compound, it is recommended to wear appropriate personal protective equipment, such as gloves, glasses and laboratory coats.
Last Update：2024-04-09 15:17:51
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CAS: 123387-72-4
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